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Drug Transporter Interaction Study PHENTRA_2015_KPUK

Registration Number
NCT02743260
Lead Sponsor
University of Cologne
Brief Summary

The objective of the present study is to contribute to establishing in vivo phenotyping procedures for organic anionic transporter polypeptide 1B1 (OATP1B1), organic cation transporters 1 and 2 (OCT1/2), multidrug and toxic compound extrusion transporters 1 and 2,kidney splice variant (MATE1/2K), organic anion transporters 1 and 3 (OAT1/3), and p-glycoprotein (P-gp) transporters via a cocktail approach. To this end, marker substrates for each of the respective transporters are administered as single doses in one period each and as a cocktail in one period to 24 healthy volunteers, and phenotyping metrics are derived from plasma and urine concentrations.

Detailed Description

Blood sampling: - 0:15 h pre-dose, 0:15, 0:30, 0:45, 1:00, 1:20, 1:40, 2:00, 2:20, 2:40, 3:00, 3:30, 4:00, 5:00, 6:00, 8:00, 12:00, 16:00, 24:00 hours post-dose

Urine Sampling: Pre-dose, 0-4 hours, 4-8 hours, 8-12 hours, 12-16 hours, 16-24 hours

Drug analysis: by liquid chromatography - tandem mass spectrometry (LC-MS/MS)

Pharmacokinetic Characteristics: Evaluation is carried out using standard noncompartmental characteristics including: area under the plasma concentration vs. time curve truncated at time t (AUC0-t), area under the plasma concentration vs. time curve extrapolated to infinity (AUC0-∞), peak plasma concentration (Cmax), time of occurrence of Cmax (tmax), apparent elimination half-life (t½), clearance over bioavailability (CL/F), renal clearance (CLr) and renal secretion. The evaluation may be completed by compartmental population pharmacokinetic approaches.

Statistical evaluation: Pharmacokinetic characteristics are compared for cocktail administration vs. individual administration by standard average bioequivalence assessment.

Safety, tolerability: Adverse events, laboratory and clinical parameters and vital signs will be assessed.

Recruitment & Eligibility

Status
COMPLETED
Sex
All
Target Recruitment
24
Inclusion Criteria
  • Caucasian
  • Body mass index (BMI) between and inclusive 18.5 and 30 kg/m2
  • Willing and capable to confirm written consent prior to enrolment after ample information has been provided
  • Normal findings in the medical history unless the principal investigator considers an abnormality to be clinically relevant.
  • Considered to be healthy by the principal investigator on the basis of extensive pre-study screening-
Exclusion Criteria

Standard for healthy volunteers, including:

  • Female subjects only: positive results in pregnancy test
  • Female subjects only: lactating women
  • Female subjects only: subjects who do not use or do not agree to use appropriate contraceptive methods during the study as defined in Note for Guidance on Non-Clinical Safety Studies for the Conduct of Human Clinical Trials for Pharmaceuticals (CHMP/ICH/286/95 modification)

Study & Design

Study Type
INTERVENTIONAL
Study Design
CROSSOVER
Arm && Interventions
GroupInterventionDescription
pitavastatin (OATP1B1)pitavastatin2 mg pitavastatin single dose
adefovir dipivoxil (OAT1)Adefovir10 mg adefovir dipivoxil single dose
cocktail (all substances)Metformincombination of all individual drugs at respective single doses
metformin (MATE1, MATE2K, OCT1, OCT2)Metformin500 mg metformin single dose
digoxin (intestinal & renal P-glycoprotein)digoxin0.5 mg digoxin single dose
sitagliptin (OAT3)sitagliptin100 mg sitagliptin single dose
cocktail (all substances)pitavastatincombination of all individual drugs at respective single doses
cocktail (all substances)digoxincombination of all individual drugs at respective single doses
cocktail (all substances)Adefovircombination of all individual drugs at respective single doses
cocktail (all substances)sitagliptincombination of all individual drugs at respective single doses
Primary Outcome Measures
NameTimeMethod
organic anionic transporter polypeptide 1B1 (OATP1B1): Clearance over bioavailability (CL/F) of pitavastatin24 hours

PK parameter

organic cation transporters 1 and 2 (OCT1/2), multidrug and toxic compound extrusion transporters 1 and 2,kidney splice variant (MATE1/2K): Renal clearance (CLr) of metformin24 hours

PK parameter

intestinal p-glycoprotein (P-gp): Peak Plasma Concentration (Cmax) of digoxin24 hours

PK parameter

renal p-glycoprotein (P-gp): Renal clearance (CLr) of digoxin:24 hours

PK parameter

organic anion transporter 1 (OAT1): Renal clearance (CLr) of adefovir24 hours

PK parameter

organic anion transporter 3 (OAT3): Renal clearance (CLr) of sitagliptin24 hours

PK parameter

Secondary Outcome Measures
NameTimeMethod

Trial Locations

Locations (1)

Department of Pharmacology I, University Hospital Cologne

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Cologne, NRW, Germany

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