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Clinical Trials/NCT02965040
NCT02965040
Completed
Phase 1

A Phase 1 Study to Evaluate the Pharmacokinetics of Roxadustat in Subjects With Different Degrees of Renal Function

Astellas Pharma Europe B.V.2 sites in 2 countries34 target enrollmentDecember 12, 2016

Overview

Phase
Phase 1
Intervention
Roxadustat
Conditions
Normal Renal Function
Sponsor
Astellas Pharma Europe B.V.
Enrollment
34
Locations
2
Primary Endpoint
Pharmacokinetics of O-glucoside-Roxadustat in plasma: TER
Status
Completed
Last Updated
6 years ago

Overview

Brief Summary

For subjects with normal renal function or severely impaired renal function, this study will evaluate the pharmacokinetics of roxadustat and its main metabolites in plasma and urine.

For subjects with end stage renal disease (ESRD) on continuous ambulatory peritoneal dialysis (CAPD) or automated peritoneal dialysis (APD), this study will evaluate the pharmacokinetics of roxadustat and its main metabolites in plasma, urine and dialysate.

For subjects with ESRD on hemodialysis (HD) or hemodiafiltration (HDF), this study will evaluate the pharmacokinetics of roxadustat and its main metabolites in plasma, urine and dialysate and also the effect of dialysis on the pharmacokinetics of roxadustat and its main metabolites.

Detailed Description

This is a phase 1, open-label study in two sites. There will be four different renal function groups. For all subjects: Subjects will be allocated to the normal and severely impaired renal function groups based on estimated glomerular filtration rate (eGFR), calculated with the abbreviated modification of diet in renal disease (MDRD) equation. The eGFR will be based on the serum creatinine concentration and is assessed at screening and at day -2. The eGFR obtained at screening will determine the allocation. Subjects will be allocated to the ESRD groups based on their dialysis requirements. Subjects with normal and severely impaired renal function, and subjects with ESRD on CAPD or APD: Screening will take place from day -30 to day -3 and the subjects will be admitted to the clinical unit on day -2. The treatment period lasts 8 days, during which the subjects will receive a single oral dose of roxadustat in the morning of day 1 Subjects will complete the treatment period on day 6, provided that all required assessments have been performed and there are no medical reasons for a prolonged follow-up. The study will be completed with an end-of-study visit (ESV), which will take place between 5 and 9 days after the last treatment period-defined assessment (or after early withdrawal). Subjects with ESRD on HD or HDF: Screening will take place from day -30 to day -3 and subjects will complete 2 treatment periods of 8 days (period 1) and 7 days (period 2) in order to evaluate the pharmacokinetics of roxadustat with a single oral dose of roxadustat on day 1 of both periods after and before dialysis. Subjects will complete the treatment period 1 on day 6 followed by a wash-out period which is minimally 1 week and maximally 3 weeks. Subjects will complete period 2 on day 6, provided that all required assessments have been performed and there are no medical reasons for a prolonged follow-up. The study will be completed with an end-of-study visit (ESV), which will take place between 5 and 9 days after the last treatment period-defined assessment (or after early withdrawal). All subjects: Safety assessments will be performed throughout the study. An optional biobanking sample may be taken for potential exploratory, retrospective, gene polymorphism analysis. Roxadustat plasma, urine, and dialysate samples will be stored for potential exploratory metabolic profiling or exploratory biomarker analysis after the study.

Registry
clinicaltrials.gov
Start Date
December 12, 2016
End Date
December 11, 2017
Last Updated
6 years ago
Study Type
Interventional
Study Design
Parallel
Sex
All

Investigators

Responsible Party
Sponsor

Eligibility Criteria

Inclusion Criteria

  • Inclusion criteria for all subjects:
  • Subject has a body weight of 45 to 160 kg, inclusive.
  • For subjects with ESRD on CAPD or APD body weight should be recorded as the measured body weight minus abdominal dialysis fluid based on the last filling. For subjects with ESRD on HD or HDF the post-dialysis body weight will be recorded.
  • Specific inclusion criteria for subjects with normal renal function:
  • Subject is a healthy male or female subject aged 40 to 75 years, inclusive.
  • Subject must have a pre-dose eGFR value based on the abbreviated MDRD method of greater than or equal to 90 mL/min/1.73 m\^
  • Specific inclusion criteria for subjects with severely impaired renal function:
  • Subject is a male or female subject aged 18 to 75 years, inclusive.
  • Subject must have a pre-dose eGFR value based on the abbreviated MDRD method \[screening\] of \<30 mL/min/1.73 m\^2 and not be on dialysis.
  • Specific inclusion criteria for subjects with ESRD on CAPD or APD:

Exclusion Criteria

  • Exclusion criteria for all subjects:
  • Subject has a known or suspected hypersensitivity to Roxadustat or any components (e.g., lactose) of the formulations used.
  • Subject has any clinically significant history of allergic conditions (including drug allergies or anaphylactic reactions, but excluding untreated, asymptomatic, seasonal allergies at time of dosing).
  • Subject has/had febrile illness or symptomatic, viral, bacterial (including upper respiratory infection), or fungal (noncutaneous) infection within 1 week prior to admission to the clinical unit.
  • Subject has any clinically significant abnormality following the investigator's review of the physical examination, electrocardiogram (ECG), and clinical study protocol-defined clinical laboratory tests at screening or day -
  • Subject has a history of smoking more than 10 cigarettes (or equivalent amount of tobacco) per day within 3 months prior to admission to the clinical unit.
  • Subject has a history of drinking more than 21 units (male subjects) or more than 14 units (female subjects) of alcohol per week (1 unit = 10 g pure alcohol = 250 mL of beer \[5%\] or 35 mL of spirits \[35%\] or 100 mL of wine \[12%\]) within 3 months prior to admission to the clinical unit.
  • Subject uses moderate or strong inducers of metabolism (e.g., barbiturates, rifampin) regularly in the 1 month prior to admission to the clinical unit.
  • Subject must not consume grapefruit (or any grapefruit-containing products, including juice) or Seville oranges (or any Seville orange-containing products, including juice) within 7 days prior to admission to the clinical unit.
  • Subject uses any drugs of abuse within 3 months prior to admission to the clinical unit.

Arms & Interventions

Roxadustat: subjects with normal renal function

Normal renal function: eGFR is equal to or greater than 90 mL/min/1.73 m\^2. Single dose of roxadustat

Intervention: Roxadustat

Roxadustat: subjects with severely impaired renal function

Severely impaired renal function: eGFR is less than 30 mL/min/1.73 m\^2. Single dose of roxadustat

Intervention: Roxadustat

Roxadustat: subjects with ESRD on CAPD or APD

ESRD subjects on CAPD or APD need to be on the same mode of dialysis for at least 4 months. Single dose of roxadustat

Intervention: Roxadustat

Roxadustat: subjects with ESRD on HD or HDF

ESRD subjects on HD or HDF need to be on the same mode of dialysis for at least 4 months and should have dialysis sessions three times weekly. Single dose of roxadustat, in both treatment periods

Intervention: Roxadustat

Outcomes

Primary Outcomes

Pharmacokinetics of O-glucoside-Roxadustat in plasma: TER

Time Frame: Up to day 6

Pharmacokinetics of Roxadustat in plasma: AUCinf,u

Time Frame: Up to day 6

AUCinf,u: Area under the concentration-time curve from the time of dosing extrapolated to time infinity for unbound concentration

Pharmacokinetics of sulfate of hydroxy-Roxadustat in plasma: AUClast

Time Frame: Up to day 6

Pharmacokinetics of Roxadustat in plasma: Vz,u/F

Time Frame: Up to day 6

Vz,u/F: Apparent volume of distribution during the terminal elimination phase of unbound compound after extravascular dosing

Pharmacokinetics of Roxadustat in plasma: Cmax

Time Frame: Up to day 6

Cmax: Maximum concentration

Pharmacokinetics of Roxadustat in plasma: Cmax,u

Time Frame: Up to day 6

Cmax,u: Maximum concentration of unbound compound

Pharmacokinetics of Roxadustat in plasma: AUCinf

Time Frame: Up to day 6

AUCinf: Area under the concentration-time curve from the time of dosing extrapolated to time infinity

Pharmacokinetics of Roxadustat in plasma: CLu/F

Time Frame: Up to day 6

CLu/F: Apparent total systemic clearance of unbound compound after extravascular dosing

Pharmacokinetics of Roxadustat in plasma: tmax

Time Frame: Up to day 6

tmax: Time of the maximum concentration

Pharmacokinetics of Roxadustat in plasma: Vz/F

Time Frame: Up to day 6

Vz/F: Apparent volume of distribution during the terminal elimination phase after single extravascular dosing

Pharmacokinetics of O-glucuronide-Roxadustat in plasma: tlag

Time Frame: Up to day 6

tlag: Time prior to the time corresponding to the first measurable (non-zero) concentration

Pharmacokinetics of O-glucoside -Roxadustat in plasma: Cmax

Time Frame: Up to day 6

Pharmacokinetics of Roxadustat in plasma: AUClast

Time Frame: Up to day 6

AUClast: Area under the concentration-time curve from the time of dosing to the last measurable concentration (Clast)

Pharmacokinetics of Roxadustat in plasma: AUClast,u

Time Frame: Up to day 6

AUClast,u: Area under the concentration-time curve from the time of dosing to the last measurable concentration (Clast) for unbound concentration

Pharmacokinetics of Roxadustat in plasma: CL/F

Time Frame: Up to day 6

CL/F: Apparent total systemic clearance after single or multiple extravascular dosing

Pharmacokinetics of Roxadustat in plasma: fu

Time Frame: Up to day 6

fu: Fraction of parent or metabolite available systemically unbound (= free fraction)

Pharmacokinetics of Roxadustat in plasma t1/2

Time Frame: Up to day 6

t1/2: Terminal elimination half-life

Pharmacokinetics of O-glucuronide-Roxadustat in plasma: Cmax

Time Frame: Up to day 6

Pharmacokinetics of O-glucuronide-Roxadustat in plasma: AUCinf

Time Frame: Up to day 6

Pharmacokinetics of O-glucuronide-Roxadustat in plasma: AUClast

Time Frame: Up to day 6

Pharmacokinetics of O-glucuronide-Roxadustat in plasma: tmax

Time Frame: Up to day 6

Pharmacokinetics of O-glucuronide-Roxadustat in plasma: t1/2

Time Frame: Up to day 6

Pharmacokinetics of O-glucuronide-Roxadustat in plasma: MPR

Time Frame: Up to day 6

MPR: Metabolite to parent ratio of AUC using AUC (corrected) for the metabolite (corrected by molecular weight ratio of parent to metabolite)

Pharmacokinetics of O-glucoside-Roxadustat in plasma: MPR

Time Frame: Up to day 6

MPR: Metabolite to parent ratio of AUC using AUC(corrected) for the metabolite (corrected by molecular weight ratio of parent to metabolite)

Pharmacokinetics of sulfate of hydroxy-Roxadustat in plasma: Cmax

Time Frame: Up to day 6

Pharmacokinetics of sulfate of hydroxy-Roxadustat in plasma: tmax

Time Frame: Up to day 6

Pharmacokinetics of O-glucoside-Roxadustat in plasma: AUCinf

Time Frame: Up to day 6

Pharmacokinetics of sulfate of hydroxy-Roxadustat in plasma: AUCinf

Time Frame: Up to day 6

Pharmacokinetics of sulfate of hydroxy-Roxadustat in plasma: tlag

Time Frame: Up to day 6

tlag: Time prior to the time corresponding to the first measurable (non-zero) concentration

Pharmacokinetics of sulfate of hydroxy-Roxadustat in plasma: t1/2

Time Frame: Up to day 6

Pharmacokinetics of Roxadustat in urine: CLR

Time Frame: Up to day 4

CLR: Renal clearance

Pharmacokinetics of O-glucoside-Roxadustat in urine: Aelast

Time Frame: Up to day 4

Pharmacokinetics of O-glucoside-Roxadustat in plasma: AUClast

Time Frame: Up to day 6

Pharmacokinetics of O-glucoside-Roxadustat in plasma: tlag

Time Frame: Up to day 6

tlag: Time prior to the time corresponding to the first measurable (non-zero) concentration

Pharmacokinetics of O-glucoside-Roxadustat in plasma: tmax

Time Frame: Up to day 6

Pharmacokinetics of O-glucoside-Roxadustat in plasma: t1/2

Time Frame: Up to day 6

Pharmacokinetics of sulfate of hydroxy-Roxadustat in plasma: MPR

Time Frame: Up to day 6

Pharmacokinetics of Roxadustat in urine: CLR,u

Time Frame: Up to day 4

CLR,u: Renal clearance of unbound drug

Pharmacokinetics of Roxadustat in urine: Aelast

Time Frame: Up to day 4

Aelast: Cumulative amount of drug excreted into urine from time of dosing up to the collection time of the last measurable concentration

Pharmacokinetics of Roxadustat in plasma: Effective t½ 56 hours

Time Frame: Up to day 6

Effective t½ 56 hours: Effective half-life based on a dosing interval of 56 hours

Pharmacokinetics of Roxadustat in urine: Aeinf

Time Frame: Up to day 4

Aeinf: Cumulative amount of compound excreted into urine from time of dosing extrapolated to time infinity

Pharmacokinetics of Roxadustat in urine: Aeinf%

Time Frame: Up to day 4

Aeinf%: Percent of drug dose excreted into urine (Aeinf) from time of dosing extrapolated to time infinity

Pharmacokinetics of Roxadustat in urine: Aelast%

Time Frame: Up to day 4

Aelast%: Percent of drug dose excreted into urine (Aelast) from time of dosing up to the collection time of the last measurable concentration

Pharmacokinetics of O-glucuronide-Roxadustat in urine: CLR

Time Frame: Up to day 4

Pharmacokinetics of O-glucuronide-Roxadustat in urine: Aeinf

Time Frame: Up to day 4

Pharmacokinetics of O-glucuronide-Roxadustat in urine: Aelast

Time Frame: Up to day 4

Pharmacokinetics of O-glucuronide-Roxadustat in urine: MPR based on Aeinf

Time Frame: Up to day 4

Pharmacokinetics of O-glucoside-Roxadustat in urine: CLR

Time Frame: Up to day 4

Pharmacokinetics of O-glucoside-Roxadustat in urine: Aeinf

Time Frame: Up to day 4

Pharmacokinetics of O-glucoside-Roxadustat in urine: MPR based on Aeinf

Time Frame: Up to day 4

Pharmacokinetics of sulfate of hydroxy-Roxadustat in urine: CLR

Time Frame: Up to day 4

Pharmacokinetics of sulfate of hydroxy-Roxadustat in urine: Aeinf

Time Frame: Up to day 4

Pharmacokinetics of sulfate of hydroxy-Roxadustat in urine: Aelast

Time Frame: Up to day 4

Pharmacokinetics of sulfate of hydroxy-Roxadustat in urine: MPR based on Aeinf

Time Frame: Up to day 4

Pharmacokinetics of O-glucoside-Roxadustat in urine: Aeinf%

Time Frame: Up to day 4

Pharmacokinetics of sulfate of hydroxy-Roxadustat in plasma: TER

Time Frame: Up to day 6

Pharmacokinetics of Roxadustat and its main metabolites in dialysate fluid: CLD

Time Frame: Up to day 2

CLD: dialysis clearance. For ESRD subjects on CAPD or APD and for ESRD subjects on HD or HDF (treatment period 2 only)

Pharmacokinetics of Roxadustat in dialysate fluid: fD

Time Frame: Up to day 2

fD: fraction of dose cleared by dialysis. For ESRD subjects on CAPD or APD and for ESRD subjects on HD or HDF (treatment period 2 only)

Pharmacokinetics of O-glucuronide-Roxadustat in urine: Aeinf%

Time Frame: Up to day 4

Pharmacokinetics of sulfate of hydroxy-Roxadustat in urine: Aeinf%

Time Frame: Up to day 4

Pharmacokinetics of Roxadustat in plasma: Effective t½ 48 hours

Time Frame: Up to day 6

Effective t½ 48 hours: Effective half-life based on a dosing interval of 48 hours

Pharmacokinetics of O-glucuronide-Roxadustat in plasma: TER

Time Frame: Up to day 6

TER: Total exposure ratio

Secondary Outcomes

  • Pharmacodynamics of Roxadustat assessed by measuring erythropoietin (EPO): AUCE,last(Up to day 6)
  • Safety assessed by nature, frequency, and severity of Adverse Events (AEs)(Up to End of Study (EOS) (Up to day 15, period 2))
  • Number of participants with vital signs abnormalities and/or adverse events related to treatment(Up to EOS (Up to day 15, period 2))
  • Pharmacodynamics of Roxadustat assessed by measuring erythropoietin (EPO): Emax-baseline(U to day 6)
  • Pharmacodynamics of Roxadustat assessed by measuring erythropoietin (EPO): Emax(Up to day 6)
  • Safety assessed by continuous heart rate (HR) measurement(Up to day 2 (period 1))
  • Number of participants with laboratory value abnormalities and/or adverse events related to treatment(Up to EOS (Up to day 15, period 2))
  • Pharmacodynamics of Roxadustat assessed by measuring erythropoietin (EPO): AUCE,last (baseline-corrected)(Up to day 6)
  • Pharmacodynamics of Roxadustat assessed by measuring erythropoietin (EPO): tmax, EPO(Up to day 6)
  • Safety assessed by routine 12- lead electrocardiogram (ECG)(Up to EOS (Up to day 15, period 2))

Study Sites (2)

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